ࡱ> 5 R)bjbjr2r2XhXh $$$$$8888pd8@XHHHH***???????$(CEn?-$*>****?$$HH ?,,,*$H$H?,*?,,7h79HWIf+(c8m??0@s8LF+jLF 7979>LF$u9**,*****??+***@****LF*********X :   Department of Energy Science, Sungkyunkwan University Suwon 16419, Republic of Korea Tel: +82-31-299-4276 Fax: +82-31-299-6505 http://shb.skku.edu/catalysis  Sustainable Technologies for the Conversion of Biomass-Derived Materials to Value-Added Chemicals Jung Woon Yang Department of Energy Science, Sungkyunkwan University, Suwon 16419, South Korea Email: jwyang@skku.edu Homepage: https://shb.skku.edu/catalysis/ The depletion of the primary energy resources such as petroleum, coal, and natural gas has been a consistent concern, thereby leading to a sharper interest in bio-based products as promising alternatives to fossil-based products.[1] Bio-refinery technologies have emerged as an environmentally friendly way to obtain bio-based products from renewable and abundant biomasses, which is expected to bring significant environmental benefits and reduce dependence on petroleum.[ ADDIN EN.CITE  ADDIN EN.CITE.DATA  HYPERLINK \l "_ENREF_1" \o "Serrano-Ruiz, 2011 #2374" 2] 2,5-Furandicarboxylic acid (FDCA) is an important renewable building block used in diverse applications such as biofuels, solvents, drugs, and biopolymer monomers in bio-refinery technologies. Herein, unique strategy for the conversion of 5-hydroxymethylfurfural (HMF) to FDCA utilizing environmentally friendly vehicles such as NaOtBu-O2 system is described, and a pilot-scale (utilizing 1 kg HMF) study is conducted to evaluate the feasibility of the mass production of FDCA (Scheme 1). In addition, a transition-metal-free chemoselective oxidative dehomologation of 2-O-benzylglycerol, which is derived from glycerol, into aromatic carboxylic acid and 2-(aryloxy)acetic acid is carried out by NaOtBu-O2 system. Furthermore, elaborative transformation of 2-(aryloxy)acetic acid to the unnatural a-amino acid is investigated using potentially infinite natural resource such as (S)-a-amino acid in combination with sodium and molecular oxygen (Scheme 2).[3] Details with the mechanistic investigation will be presented in this seminar.  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G S V X f h r w | ͹ͧޙދދދzh#hQ+hB CJOJQJ^JaJo( hQ+hQCJOJQJ^JaJh,CJOJQJ^JaJhtmCJOJQJ^JaJ#hQ+hQ+CJH*OJQJ^JaJ&hQ+hQ+6CJOJQJ]^JaJ hQ+hQ+CJOJQJ^JaJ hQ+hB CJOJQJ^JaJ hQ+haCJOJQJ^JaJ# ')*9A_` κάߞygVV hDhDCJOJQJ^JaJ#hQ+hDCJH*OJQJ^JaJ&hQ+hD6CJOJQJ]^JaJ hQ+hDCJOJQJ^JaJhDCJOJQJ^JaJhuk[CJOJQJ^JaJ&hshs6CJOJQJ]^JaJ hshsCJOJQJ^JaJhsCJOJQJ^JaJ#h#ThP,CJH*OJQJ^JaJ 6F"$468:@BN\±±{{i[JJ hQ+hDnwCJOJQJ^JaJhsCJOJQJ^JaJ#h4<h4<CJH*OJQJ^JaJ hQ+h7:eCJOJQJ^JaJ hDh7:eCJOJQJ^JaJ&h7:eh7:e6CJOJQJ]^JaJ h7:eh7:eCJOJQJ^JaJh7:eCJOJQJ^JaJhDCJOJQJ^JaJ hDhDCJOJQJ^JaJ hDhDCJOJQJ^JaJ B(5(6(7(B(XRJ4$gd84$gdgIkd$$Ifc0+P& %  t0ffffff44 lapytg$$4$Ifa$gdg4$gd/Wd4$gd/W\(( (((((((((*(0(1(2(3(4(5(6(7(~~~~~m_[V hco(hcjshghuA5U\!j)f hghuA5UV\hghuA5\jhghuA5U\jShghQY5U\!j)f hghQY5UV\Uhghc5\jhghc5U\#hQ+hd,UCJOJQJ^JaJo(hR;,CJOJQJ^JaJ hQ+hDnwCJOJQJ^JaJDocument.6.0  EMBED ChemDraw.Document.6.0  References Tuck, C. O.; Prez, E.; Horvth, I. T.; Sheldon, R. A.; Poliakoff, M. Science 2012, 337, 695. Maity, S. K. Renew. Sust. Energ. Rev. 2015, 43, 1427. Park, Y. J.; Yang, J. W. Green Chem. 2019, 21, 2615.     7(8(A(B(H(M(N(O(P(Q(V(X(Y(Z(^(_(c(h(i(j(q(r(s(x(y(z(((((((((((Ŷrch.>hnCJOJQJaJ"h.>hvO5CJOJQJ\aJ"h.>hvO6CJOJQJ]aJ h.>h/ebCJOJQJ^JaJh.>h/ebCJOJQJaJh.>hvOCJOJQJaJ h85CJOJQJ\^JaJ&h8h85CJOJQJ\^JaJ)h8h85CJOJQJ\^JaJo(#B((( ) ))))))))))gdA !$ & Fd^`a$gdn!$ & Fd<^`a$gdn ((((((((((((((((()) ) ) ) ))))⫝̸s]sNFBBFBhBjhBUh.>h.>CJOJQJaJ*h.>h.>5CJOJQJ\aJnHtH*h.>h.>6CJOJQJ]aJnHtH$h.>h.>CJOJQJaJnHtHh.>h8CJOJQJaJ$h.>h~CJOJQJaJmH sH "h.>hvO5CJOJQJ\aJ"h.>hvO6CJOJQJ]aJh.>hvOCJOJQJaJh.>h~CJOJQJaJ))))))))))h.>h.>CJOJQJaJjhBUhB 21h:pb. 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C.Luque, R.Sepulveda-Escribano, A.Univ Alicante, Lab Mat Avanzados, Alicante 03690, Spain Univ Cordoba, Dept Quim Organ, E-14014 Cordoba, SpainTransformations of biomass-derived platform molecules: from high added-value chemicals to fuels via aqueous-phase processingChemical Society ReviewsChem Soc RevChemical Society ReviewsChem Soc RevChemical Society ReviewsChem Soc Rev5266-52814011catalytic conversionsuccinic acidrenewable resourcesgamma-valerolactoneaerobic oxidationlactic-acidefficient productionethylene-glycolby-productsliquid20110306-0012WOS:000295921500005<Go to ISI>://WOS:00029592150000510.1039/c1cs15131bEnglishSheldon201423752375237517Sheldon, R. A.Delft Univ Technol, NL-2628 BL Delft, NetherlandsGreen and sustainable manufacture of chemicals from biomass: state of the artGreen ChemistryGreen ChemGreen ChemistryGreen ChemGreen ChemistryGreen Chem950-963163ionic liquid pretreatmentgamma-valerolactoneorganic-synthesislevulinic acidrenewable resourcesescherichia-coliselective hydrogenationlignocellulosic biomassfermentative productionenzymatic-hydrolysis20141463-9262WOS:000332039200001<Go to ISI>://WOS:00033203920000110.1039/c3gc41935eEnglishMaity201523772377237717Maity, S. K.Indian Inst Technol Hyderabad, Dept Chem Engn, Yeddumailaram 502205, Telangana, IndiaOpportunities, recent trends and challenges of integrated biorefinery: Part IRenewable & Sustainable Energy ReviewsRenew Sust Energ RevRenewable & Sustainable Energy ReviewsRenew Sust Energ RevRenewable & Sustainable Energy ReviewsRenew Sust Energ Rev1427-144543biorefinerybiomassbio-fuelsplatform chemicallignocellulosestarchcatalytic conversionlignocellulosic biomasshydrogen-productionbio-oilbiotechnological productionhydrothermal liquefactionfermentative productionmicrobial-productionrenewable resourcesanaerobic-digestion2015Mar1364-0321WOS:000348880600108<Go to ISI>://WOS:00034888060010810.1016/j.rser.2014.11.092EnglishTakkellapati201823802380238017Takkellapati, S.Li, T.Gonzalez, M. A.US EPA, Natl Risk Management Res Lab, Off Res & Dev, Cincinnati, OH 45268 USAAn overview of biorefinery-derived platform chemicals from a cellulose and hemicellulose biorefineryClean Technologies and Environmental PolicyClean Technol EnvirClean Technologies and Environmental PolicyClean Technol EnvirClean Technologies and Environmental PolicyClean Technol Envir1615-1630207biorefinerybiomassplatform chemicalslignocellulosegasificationfermentationlignocellulosic biomasslactic-acidrenewable resourceslevulinic acidglycerolconversionefficientpretreatmentchallengesoxidation2018Sep1618-954xWOS:000441735600020<Go to ISI>://WOS:00044173560002010.1007/s10098-018-1568-5EnglishCorma200723922392239217Corma, A.Iborra, S.Velty, A.Univ Politecn Valencia, CSIC, Inst Tecnol Quim, E-46071 Valencia, SpainChemical routes for the transformation of biomass into chemicalsChemical ReviewsChem RevChemical ReviewsChem RevChemical ReviewsChem Rev2411-25021076liquid-phase hydrogenationalpha-pinene oxidefatty-acid estersplatinum-catalyzed oxidationamorphous alloy catalystsupported aqueous-phaserenewable raw-materialsone-pot synthesisrhodium hydroformylation catalystssurface organometallic chemistry2007Jun0009-2665WOS:000247217000012<Go to ISI>://WOS:00024721700001210.1021/cr050989dEnglish)Fernando200623842384238417Fernando, S.Adhikari, S.Chandrapal, C.Murali, N.Mississippi State Univ, Dept Agr & Biol Engn, Mississippi State, MS 39762 USABiorefineries: Current status, challenges, and future directionEnergy & FuelsEnerg FuelEnergy & FuelsEnerg FuelEnergy & FuelsEnerg Fuel1727-1737204catalytic hydrotreatmentpyrolysishydrodeoxygenation2006Jul 190887-0624WOS:000239120000053<Go to ISI>://WOS:00023912000005310.1021/ef060097wEnglishSerrano-Ruiz201123742374237417Serrano-Ruiz, J. C.Luque, R.Sepulveda-Escribano, A.Univ Alicante, Lab Mat Avanzados, Alicante 03690, Spain Univ Cordoba, Dept Quim Organ, E-14014 Cordoba, SpainTransformations of biomass-derived platform molecules: from high added-value chemicals to fuels via aqueous-phase processingChemical Society ReviewsChem Soc RevChemical Society ReviewsChem Soc RevChemical Society ReviewsChem Soc Rev5266-52814011catalytic conversionsuccinic acidrenewable resourcesgamma-valerolactoneaerobic oxidationlactic-acidefficient productionethylene-glycolby-productsliquid20110306-0012WOS:000295921500005<Go to ISI>://WOS:00029592150000510.1039/c1cs15131bEnglishSheldon201423752375237517Sheldon, R. A.Delft Univ Technol, NL-2628 BL Delft, NetherlandsGreen and sustainable manufacture of chemicals from biomass: state of the artGreen ChemistryGreen ChemGreen ChemistryGreen ChemGreen ChemistryGreen Chem950-963163ionic liquid pretreatmentgamma-valerolactoneorganic-synthesislevulinic acidrenewable resourcesescherichia-coliselective hydrogenationlignocellulosic biomassfermentative productionenzymatic-hydrolysis20141463-9262WOS:000332039200001<Go to ISI>://WOS:00033203920000110.1039/c3gc41935eEnglishMaity201523772377237717Maity, S. K.Indian Inst Technol Hyderabad, Dept Chem Engn, Yeddumailaram 502205, Telangana, IndiaOpportunities, recent trends and challenges of integrated biorefinery: Part IRenewable & Sustainable Energy ReviewsRenew Sust Energ RevRenewable & Sustainable Energy ReviewsRenew Sust Energ RevRenewable & Sustainable Energy ReviewsRenew Sust Energ Rev1427-144543biorefinerybiomassbio-fuelsplatform chemicallignocellulosestarchcatalytic conversionlignocellulosic biomasshydrogen-productionbio-oilbiotechnological productionhydrothermal liquefactionfermentative productionmicrobial-productionrenewable resourcesanaerobic-digestion2015Mar1364-0321WOS:000348880600108<Go to ISI>://WOS:00034888060010810.1016/j.rser.2014.11.092EnglishTakkellapati201823802380238017Takkellapati, S.Li, T.Gonzalez, M. A.US EPA, Natl Risk Management Res Lab, Off Res & Dev, Cincinnati, OH 45268 USAAn overview of biorefinery-derived platform chemicals from a cellulose and hemicellulose biorefineryClean Technologies and Environmental PolicyClean Technol EnvirClean Technologies and Environmental PolicyClean Technol EnvirClean Technologies and Environmental PolicyClean Technol Envir1615-1630207biorefinerybiomassplatform chemicalslignocellulosegasificationfermentationlignocellulosic biomasslactic-acidrenewable resourceslevulinic acidglycerolconversionefficientpretreatmentchallengesoxidation2018Sep1618-954xWOS:000441735600020<Go to ISI>://WOS:00044173560002010.1007/s10098-018-1568-5EnglishCorma200723922392239217Corma, A.Iborra, S.Velty, A.Univ Politecn Valencia, CSIC, Inst Tecnol Quim, E-46071 Valencia, SpainChemical routes for the transformation of biomass into chemicalsChemical ReviewsChem RevChemical ReviewsChem RevChemical ReviewsChem Rev2411-25021076liquid-phase hydrogenationalpha-pinene oxidefatty-acid estersplatinum-catalyzed oxidationamorphous alloy catalystsupported aqueous-phaserenewable raw-materialsone-pot synthesisrhodium hydroformylation catalystssurface organometallic chemistry2007Jun0009-2665WOS:000247217000012<Go to ISI>://WOS:00024721700001210.1021/cr050989dEnglish Dd b  c $A? ?3"`?"" @`.4r~bw;TSp=@=@`.4r~bw;  !"#$%&'()*+,-./0123456789:;<=>?@ABCDEFGHIJKLMNOPQRSTUVWXYZ[\]^_`abcdefghijklmnopqrstuvwxyz{|}~      !"#$%&'()*+,-./0123456789:;<=>?@ABCDEFGHIJKLMNOPQRSTUVWYZ[\]^_`abcdefghijklmnopqrstuvwxyz{|}~Root Entry FWI Data XWordDocumentObjectPool:WIWI_1724066077 !mA. :WIrWIOle CompObj~ObjInfo  !# !mA. 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